UWM Logo
 		 Department of Chemistry
NMR facility 		fourier transform

CHEMISTRY 781: Nuclear Magnetic Resonance Spectroscopy: Theory and Practice (Semester 1, Fall 2004)
  • Syllabus
  • Tenative Course Outline
  • Topics for student presentations
  • Lecturenotes (PDF-format)
  • Handouts
  • Solutions to labs, exams and practice questions

    • Chem 781 In class presentations:

    Each student chooses one of the listed research articles and explains it to the class on the date indicated as a 20 min presentation. The presentation is expected to contain both the specific application mentioned in the article and a more general description of the NMR method applied which may require the use of additional articels mentioned in the paper. Presentations must be discussed with the instructor at least a week prior to the scheduled date.

  • -1H-NMR without deuterated solvents (10/14): Huili Yao
    Thomas R. Hoye, Brian M. Eklov, and Mikhail Voloshin "No-D NMR Spectroscopy as a Convenient Method for Titering Organolithium (RLi), RMgX, and LDA Solutions" Org. Lett. 2004 6(15) 2567-2570 and relevant references therein



  • -Analyzing multiplet patterns (10/14): Karen Crozier
    Thomas R. Hoye and Hongyu Zhao; "A Method for Easily Determining Coupling Constant Values: An Addendum to 'A Practical Guide to First-Order Multiplet Analysis in 1H NMR Spectroscopy' "; J. Org. Chem. 2002, 67, 4014-4016 and references therein

  • -Sensitivity enhancement of low- nuclei(10/19): Chris McCullough
    B. Wrackemeyer, O. L. Tok, M.Herberhold; "57Fe NMR of Ferrocenes by 1H-57Fe INEPT Techniques" Organometallics 2001, 20 (26), 5774 -5776

  • -Application of 15 N correlation spectroscopy I(11/2): Christine Carlson "Facile Determination of the Protecting Group Location of Nim-Protected Histidine Derivatives by 1H-15N Heteronuclear Correlation NMR Simone Zaramella, Petri Heinonen, Esther Yeheskiely, and Roger Strömberg J. Org. Chem. 2003, 68, 7521-7523 OR

  • -Application of 15 N correlation spectroscopy II(11/2): Chris Oberle
    Damblon, C.; Prosperi, C.; Lian, L.-Y.; Barsukov, I.; Soto, R. P.; Galleni, M.; Frere, J.-M.; Roberts, G. C. K.; "1H-15N HMQC for the Identification of Metal-Bound Histidines in 113Cd-Substituted Bacillus cereus Zinc -Lactamase "; J. Am. Chem. Soc. 1999, 121(49), 11575-11576.

  • -Automated structure elucidation:(11/2) Michael Van Linn Jochen Junker, Walter Maier, Thomas Lindel, and Matthias Köck; "Computer-Assisted Constitutional Assignment of Large Molecules: COCON Analysis of Ascomycin " Org. Lett., 1(5), 1999, 737-740 also briefly mention
    Köck M, Junker J, Lindel T; "Impact of the H-1,N-15-HMBC experiment on the constitutional analysis of alkaloids"; Org. Lett. 1999, 1 (13), 2041-2044

  • - Multidimensional NMR of 183W and 51V (11/4): Luke Hergert
    Domaille, P. J.; "The one- and Two-Dimensional Tungsten-183 and Vanadium-51 NMR characterization of isopolymetalates and heteropolymetalates" J. Am. Chem. Soc. 1984, 106, 7677-7687.
    • bar.gif
    To Top of This Page Back to NMR Home To Chemistry Main Page To UWM Home
    bar.gif
    This page was last updated by Holger Försterling on Monday, 30-Apr-2007 15:15:36 CDT