Standard Experiments available on the DPX300

use command rpar parameter_file all
Pameter file description Phasing Time
(default parameters)
1D 1H and 13C:
h1.hf 1D standard Proton, 16 scans   1 min
c13.hf 1D standard C-13, 1024 scans   34 min
carbonsave.hf 1D long term carbon, saves every 1024 scans: 24*1024 scans   13 h 50 min
c13gatdec.hf 1D C-13, proton coupled   1 h 30 min
c13invgat.hf 1D carbon, no NOE, for quantitative integrations   2 h 40 min
c13dept135.hf 1D C-13 DEPT-135, CH and CH3 up, CH2down   10 min
c13dept90.hf 1D 13C DEPT-90, CH only   10 min
watergate.hf 1D proton with water supression   5 min
noe1d.hf 1D gradient selected transient NOE experiment, use special instructions   30 min
roe1d.hf 1D ROE experiment, set up like 1D NOE   30 min
tocsy1d.hf 1D selective TOCSY experiment, set up like 1D NOE   1 min
2D (1H/1H):
quickcosy.hf 2D 1H/1H COSY, for concentrated samples 1 scan per increment, minimum resolution no 4 min
cosy.hf 2D 1H/1H COSY no 15 min
cosydqf.hf 2D H/H COSY with double quantum filter for measurement of H/H couplings and diagonal supression yes 45 min
pecosy.hf 2D H/H P.E. COSY ,simplified crosspeaks for coupling constant measurement and diagonal supression yes 1 h30 min
tocsy.hf 2D 1H/1H total correlation (TOCSY) tmix = 60ms yes 20 min
roesy.hf 2D 1H/1H ROESY (through space correlation for M300-1000) tmix = 400 ms yes 1 h 16 min
noesy.hf 2D 1H/1H NOESY (through space correlation) default mixing time d8 = 400ms yes 1 h 16 min
2D(1H/13C):
hsqc.hf 2D 1H/13C one bond correlation (HSQC) yes 8 min
hsqc_ed.hf 2D 1H/13C one bond correlation with editing: CH,CH3 positive, CH2 negative yes 18min
hmbc.hf 2D 1H/13C multiple (2-3) bond correlation no 1 h 30 min
hsqctocsy.hf 2D 1H{13C} correlation with 1H-1H TOCSY yes 1h 16 min
X and 1H/X experiments:
b11.hf 1D 11B   15 min
b11hsqc.hf 2D 1H{11B} correlation yes 16 min
f19.hf 1D 19F, recabeling required, see special instructions   1 min
n14.hf 1D 14N   25 min
n15hsqc.hf 2D 1H/15N correlation yes 1h 20 min
si29.hf 1D 29Si   3h 50 min
sn119.hf 1D 119Sn
p31.hf 1D 31P with 1H decoupling   5 min
p31_cosy.hf 2D 31P/31P correlation (COSY) no 5h
p31_hmbc.hf 2D 1H/31P correlation no 43 min

Last update: -->October 22, 2004